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Information
| Code | KM236 |
| Name | Organic Chemistry Lab. 2 |
| Term | 2022-2023 Academic Year |
| Semester | 4. Semester |
| Duration (T+A) | 0-4 (T-A) (17 Week) |
| ECTS | 3 ECTS |
| National Credit | 2 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Prof. Dr. ELİFE SULTAN GİRAY |
| Course Instructor |
Prof. Dr. ELİFE SULTAN GİRAY
(A Group)
(Ins. in Charge)
Öğr. Gör.Dr. ONUR DEMİRKOL (A Group) (Asst. Ins.) |
Course Goal / Objective
Understanding the basic purification methods and establishing some basic organic reaction mechanisms, obtaining the product, determining the structure by product purification and FTIR analysis
Course Content
The basic purification methods used in Organic Chemistry and applications of some organic reactions
Course Precondition
none
Resources
Experimental Organic Chemistry Ender Erdik
Notes
Organic Chemistry T. W. Graham Solomons, Craig B. Fryhle, Scott A. Snyder
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | m-dinitrobenzene synthesizes, purifies and determines its structure by FTIR spectroscopy |
| LO02 | Synthesizes the 2,4-dinitro-1-naphthol compound, at the same time, comprehends both the sulfation and nitration reactions, purifies the product and illuminates its structure. |
| LO03 | Synthesize p-benzoquinone, understand oxidation reactions, make product purification and structure determination |
| LO04 | Synthesis Ethyl acetate, learns the esterification reactions, purifies the product and illuminates its structure |
| LO05 | Synthesizes benzoin, learns condensation reactions, purifies the product and brightens its structure |
| LO06 | Performs Compensation Experiments. |
| LO07 | comprehend chromatographic methods. |
| LO08 | Synthesize Coumarin compounds, learn condensation reactions, purify the product and brighten its structure |
| LO09 | Synthesizes the chalcone compound, learns the condensation reactions, purifies the product and brightens its structure. |
| LO10 | Can synthesize phthalimide, purifies the product and brightens its structure. |
| LO11 | Can synthesize adipic acid, learn oxidation reactions, purify the product and brighten its structure |
| LO12 | Can do dyestuff synthesis, learn coupling reactions, purify the product and brighten its structure |
| LO13 | Comprehends the safety precautions to be applied while working in the laboratory. |
| LO14 | Comprehends the safety and first aid information to be applied against the chemicals to be used in the experiments. |
| LO15 | Understands and applies separation techniques |
| LO16 | Learns to use glass materials necessary to set up experiments |
| LO17 | Understands which separation technique should be used to separate the product obtained at the end of the experiment from the environment. |
| LO18 | Understands and applies the rules to be followed while working in the laboratory |
| LO19 | comprehend and apply purification techniques. |
| LO20 | understands what to do in case of an accident in the laboratory. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Relates his/her knowledge in the field of chemistry to life and industry by relying on his/her knowledge | 4 |
| PLO02 | Bilgi - Kuramsal, Olgusal | Evaluates the developments in the world by following and perceiving the orientations in the industry. | 3 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Gains awareness of lifelong learning and renews his/her knowledge. | |
| PLO04 | Bilgi - Kuramsal, Olgusal | Access to information and associate their knowledge with other fields of science. | |
| PLO05 | Bilgi - Kuramsal, Olgusal | Understands the need to combine information in the application of information and perceives the total quality awareness. | 2 |
| PLO06 | Bilgi - Kuramsal, Olgusal | S/he has knowledge in the use of resources, in the creation of technology depending on the country's resources. | 2 |
| PLO07 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | S/he conveys what s/he knows to people close or distant to the subject by concretising. | |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Gains the ability to access new information and technology. | 3 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Learns to think creatively and produce solutions to problems in the field. | 5 |
| PLO10 | Yetkinlikler - Öğrenme Yetkinliği | To be able to associate information by having the ability of reasoning and transfer what they know to practice. | 2 |
| PLO11 | Beceriler - Bilişsel, Uygulamalı | Sets up laboratory equipment and makes decisions alone. | 5 |
| PLO12 | Bilgi - Kuramsal, Olgusal | To be able to follow the current technology in the field of chemistry and gain added value. | 4 |
| PLO13 | Bilgi - Kuramsal, Olgusal | Follows the developments, gains the ability to follow the directions in the field. | 5 |
| PLO14 | Bilgi - Kuramsal, Olgusal | Knowing information sharing and participating in teamwork and directing the team. | 4 |
| PLO15 | Beceriler - Bilişsel, Uygulamalı | Gains universal thinking and critical perspective. | 4 |
| PLO16 | Bilgi - Kuramsal, Olgusal | Starts to have a say in the field. | 5 |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Synthesis of m-dinitrobenzene | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 2 | Synthesis of 2,4-dinitro-1-naphthol | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 3 | Synthesis of p-benzoquinone | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 4 | Synthesis of ethylacetate | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 5 | Synthesis of benzoin | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 6 | compensating experiments-1 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 7 | compensating experiments-2 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 8 | Mid-Term Exam | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 9 | Synthesis of coumarin | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 10 | Synthesis of chalcone | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 11 | synthesis of phthalimide | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 12 | Syntesis of adipic acid | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 13 | dyestuff synthesis | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 14 | compensating experiments-3 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 15 | compensating experiments-4 | Experimental Organic Chemistry Ender Erdik | Öğretim Yöntemleri: Deney / Laboratuvar |
| 16 | Term Exams-1 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams-2 | Experimental Organic Chemistry Ender Erdik | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 0 | 0 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 12 | 12 |
| Final Exam | 1 | 24 | 24 |
| Total Workload (Hour) | 64 | ||
| Total Workload / 25 (h) | 2,56 | ||
| ECTS | 3 ECTS | ||