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Information
| Code | ECF209 |
| Name | Analytical Chemistry Laboratory II |
| Term | 2022-2023 Academic Year |
| Semester | 3. Semester |
| Duration (T+A) | 0-3 (T-A) (17 Week) |
| ECTS | 2 ECTS |
| National Credit | 1.5 National Credit |
| Teaching Language | Türkçe |
| Level | Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | Dr. Öğr. Üyesi SABRİYE AYDINOĞLU |
| Course Instructor |
Dr. Öğr. Üyesi SABRİYE AYDINOĞLU
(A Group)
(Ins. in Charge)
Dr. Öğr. Üyesi Merve NENNİ (A Group) (Asst. Ins.) Prof. Dr. Hacı Ali DÖNDAŞ (A Group) (Asst. Ins.) Dr. Öğr. Üyesi SABRİYE AYDINOĞLU (B Group) (Ins. in Charge) Dr. Öğr. Üyesi Merve NENNİ (B Group) (Asst. Ins.) Prof. Dr. Hacı Ali DÖNDAŞ (B Group) (Asst. Ins.) |
Course Goal / Objective
The student is expected to become familiar with the instrumental analysis methods, their basis and potential use.
Course Content
Learning of electrochemical, spectrochemical and chromatographic analysis methods and validation parameters
Course Precondition
None
Resources
Aydinoglu S., Alptekin Ö., Secco F., Analytical Chemistry Laboratory II Text Book, Cukurova University Pharmacy Department
Notes
Aydinoglu S., Alptekin Ö., Secco F., Analytical Chemistry Laboratory II Text Book, Cukurova University Pharmacy Department
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Knowledge of conductivity titration acquires application skills in complex acid base systems. |
| LO02 | Understands the principles of potentiometric titration and uses it to calculate the equilibrium constants of a polyprotic acid or base. |
| LO03 | Be able to perform UV-GB spectroscopy in order to quantitative the analysis of mixtures. |
| LO04 | Be able to perform thin layer chromatography to do qualitative analysis. |
| LO05 | Be able to do quantitative analysis by refractometry |
| LO06 | Perform derivative spectrophotometry methods for quantitative analysis of pharmaceutial mixture |
| LO07 | Could be perform atomic absorption spectroscopy for quantitative analysis. |
| LO08 | Be able to perform column chromatography. |
| LO09 | Explain the basic principles of high performance liquid chromatography. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Have sufficient knowledge in pharmaceutical field and develop the knowledge. | 3 |
| PLO02 | Bilgi - Kuramsal, Olgusal | Comprehends professional knowledge with ethical responsibility through current laws and legislation. | 2 |
| PLO03 | Beceriler - Bilişsel, Uygulamalı | Provides consultancy service to patients, community and health care personnel and evaluates advanced knowledge and skills with a critical approach. | |
| PLO04 | Beceriler - Bilişsel, Uygulamalı | Possessing the knowledge of historical and current developments in the field of Pharmacy, monitoring, evaluation and application of scientific and evidence-based data, and adopting lifelong learning. | 4 |
| PLO05 | Beceriler - Bilişsel, Uygulamalı | Have the knowledge and skills to help provide patient-oriented pharmacy applications and individualized pharmaceutical care by learning the basics of Clinical Pharmacy, | |
| PLO06 | Yetkinlikler - Bağımsız Çalışabilme ve Sorumluluk Alabilme Yetkinliği | Takes a role in the evaluation and analysis of the events and cases related to the development of pharmacy profession and education. | |
| PLO07 | Yetkinlikler - Öğrenme Yetkinliği | Integrates and develops professional knowledge via different disciplines and uses the acquired knowledge to improve the health level and quality of life of the community. | 3 |
| PLO08 | Yetkinlikler - Öğrenme Yetkinliği | Use effectively the concepts and applications of basic sciences and basic medical sciences in the field of medicine and pharmacy and update the information. | 4 |
| PLO09 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Communicates effectively in writing and speaking. | 3 |
| PLO10 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Practices the profession in accordance with Atatürk's principles and reforms, equipped with universal knowledge, uses Turkish correctly and knows at least one foreign language. | |
| PLO11 | Yetkinlikler - İletişim ve Sosyal Yetkinlik | Be an example to society withexternal appearance, demeanor, attitude and behavior for the other professionals and society and with professional identity | |
| PLO12 | Yetkinlikler - Alana Özgü Yetkinlik | Have knowledge about health policies and health economics, pharmacy management and define the problems in pharmaceutical field. | |
| PLO13 | Yetkinlikler - Alana Özgü Yetkinlik | Interprets information about current health and treatment problems and attends meeting on related matters . Plays an active role in community health. | |
| PLO14 | Yetkinlikler - Alana Özgü Yetkinlik | Acquires basic information about diseases, makes decisions about the drugs used in treatment in accordance with rational drug use. |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Introduction of spectroscopic, chromatographic and electrochemical analysis methods | Quiz and Report | Öğretim Yöntemleri: Anlatım, Tartışma, Soru-Cevap, Örnek Olay |
| 2 | Conductivity analysis of strong and weak acids | Quiz and Report | Öğretim Yöntemleri: Anlatım, Deney / Laboratuvar, Grup Çalışması |
| 3 | Potentiometric titration of polyprotic acids or bases | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Deney / Laboratuvar, Grup Çalışması |
| 4 | Spectrophotometric determination of two-component mixtures | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Gösterip Yaptırma, Bireysel Çalışma |
| 5 | Analysis of binary mixtures by differential UV spectrophotometry | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Alıştırma ve Uygulama, Grup Çalışması, Deney / Laboratuvar |
| 6 | Determination of complex formulas and stability constants by spectrophotometric method | Quiz and Report | Öğretim Yöntemleri: Soru-Cevap, Anlatım, Tartışma, Deney / Laboratuvar, Problem Çözme |
| 7 | Mixture analysis by spectrophotometric titration | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Gösterip Yaptırma, Beyin Fırtınası, Deney / Laboratuvar |
| 8 | Mid-Term Exam | Literature Search and Related Calculations | Ölçme Yöntemleri: Ödev, Performans Değerlendirmesi |
| 9 | Introduction to Validation | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma |
| 10 | Qualitative analysis of drugs by thin layer chromatography | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Gösterip Yaptırma, Grup Çalışması, Deney / Laboratuvar |
| 11 | Separation of indicator mixtures by column chromatography | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Gösterip Yaptırma, Deney / Laboratuvar |
| 12 | Quantitative analysis by high performance liquid chromatography | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Gösterip Yaptırma, Deney / Laboratuvar |
| 13 | Cation analysis by atomic absorption spectroscopy | Quiz and Report | Öğretim Yöntemleri: Soru-Cevap, Anlatım, Gösterip Yaptırma, Grup Çalışması, Deney / Laboratuvar |
| 14 | Kinetic Determination of Trace Copper | Quiz and Report | Öğretim Yöntemleri: Anlatım, Soru-Cevap, Tartışma, Gösterip Yaptırma, Deney / Laboratuvar, Grup Çalışması |
| 15 | Validation Study | Presentation | Öğretim Yöntemleri: Soru-Cevap, Tartışma, Grup Çalışması, Beyin Fırtınası, Örnek Olay |
| 16 | Term Exams | General Ripetition | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams | General Ripetition | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 1 | 14 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 2 | 28 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 3 | 3 |
| Final Exam | 1 | 9 | 9 |
| Total Workload (Hour) | 54 | ||
| Total Workload / 25 (h) | 2,16 | ||
| ECTS | 2 ECTS | ||