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Information
| Code | FK0053 |
| Name | Structural and Magnetic Characterization Techniques-I |
| Term | 2024-2025 Academic Year |
| Term | Fall |
| Duration (T+A) | 3-0 (T-A) (17 Week) |
| ECTS | 6 ECTS |
| National Credit | 3 National Credit |
| Teaching Language | Türkçe |
| Level | Yüksek Lisans Dersi |
| Type | Normal |
| Mode of study | Yüz Yüze Öğretim |
| Catalog Information Coordinator | |
| Course Instructor |
Doç. Dr. Selda KILIÇ ÇETİN
(A Group)
(Ins. in Charge)
|
Course Goal / Objective
The aim of this course is to teach the crystal structure and lattice parameters of materials, crystal structure determination, teaching XRD diffraction technique, explaining imaging techniques, teaching magnetic measurement systems.
Course Content
Structural properties of materials, Crystal structure and lattice parameters, Determination of crystal structure with XRD technique, Elemental analysis and surface morphology examination with SEM/EDX measurement techniques, PPMS system and measurement options, Magnetization measurements depending on temperature and magnetic field with VSM option.
Course Precondition
There are no course prerequisites.
Resources
X-Ray Diffraction, Cullity
Notes
Lecture notes
Course Learning Outcomes
| Order | Course Learning Outcomes |
|---|---|
| LO01 | Defines the structural properties of materials. |
| LO02 | Learns about the crystal structure. |
| LO03 | Defines the crystal structure parameters. |
| LO04 | Knows the application areas of XRD diffraction method. |
| LO05 | Calculate the crystal structure of a material from XRD data. |
| LO06 | Learns about the working principle of scanning electron microscope. |
| LO07 | Interpret scanning electron microscope images. |
| LO08 | Defines the working principle of the EDS system. |
| LO09 | Calculate the formulation of the material from the EDS data. |
| LO10 | Learns about the magnetic properties of materials. |
Relation with Program Learning Outcome
| Order | Type | Program Learning Outcomes | Level |
|---|---|---|---|
| PLO01 | Bilgi - Kuramsal, Olgusal | Has sufficient infrastructure in various subjects of Physics. | |
| PLO02 | Bilgi - Kuramsal, Olgusal | Demonstrate the knowledge of appropriate mathematical techniques used in physics. | 2 |
| PLO03 | Bilgi - Kuramsal, Olgusal | Interpret observational and experimental results. | 4 |
| PLO04 | Bilgi - Kuramsal, Olgusal | Makes use of the conceptual and practical knowledge acquired in the physics field at mastery level. | 3 |
| PLO05 | Bilgi - Kuramsal, Olgusal | Has a knowledge about the logic of scientific research. | 3 |
| PLO06 | Bilgi - Kuramsal, Olgusal | Report the solution of a physics problem, experimental results or projects in a written format or orally. | 3 |
| PLO07 | Bilgi - Kuramsal, Olgusal | Chooses and uses the necessary publications, books and methods for a scientific research. | 2 |
| PLO08 | Bilgi - Kuramsal, Olgusal | Accesses a knowledge about a subject in physics, does literature search and uses other sources for this purpose. | 3 |
| PLO09 | Bilgi - Kuramsal, Olgusal | Provides solutions to the problems encountered in the physics field applying research methods. | 3 |
| PLO10 | Bilgi - Kuramsal, Olgusal | Can perform an independent research. | |
| PLO11 | Bilgi - Kuramsal, Olgusal | Can perform group work effectively in a research or industrial projects. | |
| PLO12 | Bilgi - Kuramsal, Olgusal | Becomes conscious of the necessity of lifelong learning. | |
| PLO13 | Bilgi - Kuramsal, Olgusal | To keep track of the developments in physics and updates himself/herself invariably. | 3 |
| PLO14 | Bilgi - Kuramsal, Olgusal | Shares his/her ideas and suggestions for solutions to the physical problems with experts and non-experts by supporting them with quantitative and qualitative data. | |
| PLO15 | Bilgi - Kuramsal, Olgusal | Can make an effective written or oral presentation of the results obtained in a study. | 4 |
| PLO16 | Bilgi - Kuramsal, Olgusal | Makes use of the knowledge, problem solving and / or application skills acquired in the physics field in interdisciplinary studies. | 3 |
| PLO17 | Bilgi - Kuramsal, Olgusal | Has a foundation necessary to work in a research and development organizations. |
Week Plan
| Week | Topic | Preparation | Methods |
|---|---|---|---|
| 1 | Crystal structure | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 2 | Crystal lattice parameters | Preparation and reading different sources | Öğretim Yöntemleri: Soru-Cevap, Anlatım |
| 3 | XRD diffraction technique | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 4 | Structure determination by XRD diffraction technique | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 5 | Working Principle of Scanning Electron Microscope | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 6 | EDS working principle | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 7 | Interpretation of SEM/EDS results | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 8 | Mid-Term Exam | Ölçme Yöntemleri: Ödev |
|
| 9 | Introduction to magnetism | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 10 | Classification of Magnetic Materials | Preparation and reading different sources | Öğretim Yöntemleri: Soru-Cevap, Anlatım |
| 11 | Working principle of VSM system | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 12 | Temperature dependent magnetization measurements | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 13 | Field dependent magnetization measurements | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 14 | Plotting magnetization graphs from VSM results | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 15 | Interpretation of magnetization graphs | Preparation and reading different sources | Öğretim Yöntemleri: Anlatım, Soru-Cevap |
| 16 | Term Exams | Preparation for exam | Ölçme Yöntemleri: Yazılı Sınav |
| 17 | Term Exams | Preparation for exam | Ölçme Yöntemleri: Yazılı Sınav |
Student Workload - ECTS
| Works | Number | Time (Hour) | Workload (Hour) |
|---|---|---|---|
| Course Related Works | |||
| Class Time (Exam weeks are excluded) | 14 | 3 | 42 |
| Out of Class Study (Preliminary Work, Practice) | 14 | 5 | 70 |
| Assesment Related Works | |||
| Homeworks, Projects, Others | 0 | 0 | 0 |
| Mid-term Exams (Written, Oral, etc.) | 1 | 15 | 15 |
| Final Exam | 1 | 30 | 30 |
| Total Workload (Hour) | 157 | ||
| Total Workload / 25 (h) | 6,28 | ||
| ECTS | 6 ECTS | ||